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Chemical Reference Materials: Setting the Standards for Ocean Science
APPENDIX E
Reference Materials Listed within this Report
Any current comprehensive, printed, list of reference materials for ocean science would quickly become obsolete as new materials are produced and others go out of stock. Perhaps the most complete list produced to date is that assembled by Dr. Adrianna Cantillo of the NOAA Status and Trends Program:
Cantillo, A.Y. 1995. Standard and Reference Materials for Environmental Science (Part 1 and Part 2). NOAA Technical Memo. 94. NOAA/ NOS/ORCA, Silver Spring, MD. 752 pp.
Another list of environmentally relevant reference materials is maintained at the IAEA web-site (http://www.iaea.or.at/programmes/nahunet/e4/nmrm/). Nevertheless, new materials are produced each year, and older ones run out and are not replaced so it is important to keep such lists current.
Clearly this is an arena in which computer database technology has a major role to play. Perhaps the best developed such database is COMAR (an index Code of Reference Materials). This database tries to provide an up-to-date way to locate CRMs from all around the world. The Central Secretariat is presently housed at the Federal Institute for Materials Research and Testing (BAM), Berlin, Germany. Further information is available at the COMAR website (http://www.comar.bam.de/). Nevertheless, this database is not restricted to ocean science applications (indeed
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Chemical Reference Materials: Setting the Standards for Ocean Science
they represent a very small fraction of available reference materials), and is not particularly user-friendly.
There is thus a need for a searchable, ocean science specific, database of currently available reference materials, and one of the recommendations of this report is that such a database be developed and maintained by the ocean science community.
Reference materials cited in this report, currently available for use in ocean science.
Identifier
Matrix
Analyzed For
Source (see footnotes)
Ocean CO2 RMs
Natural Seawater
Total Dissolved Inorganic carbon, Total Alkalinty
Dr. A. G. Dickson, U.C. San Diego(1)
DOC-CRM
Natural Seawater
Dissolved Organic Carbon
Dr. D. Hansell, U. Miami(2)
FIRI A, B (†)
Kauri Wood
pMC
Dr. E. M. Scott, U. Glasgow (3)
FIRI C
Turbidite Carbonate
pMC
Dr. E. M. Scott, U. Glasgow
FIRI E
Humic Acid
pMC
Dr. E. M. Scott, U. Glasgow
FIRI G, J
Barley Mash
pMC
Dr. E. M. Scott, U. Glasgow
FIRI H
German Oak Dendro-dated Wood
pMC
Dr. E. M. Scott, U. Glasgow
FIRI I
Belfast Scots Pine Dendro-dated Wood Cellulose
pMC
Dr. E. M. Scott, U. Glasgow
FIRI K
Cambridge Dendro-wood Whole Wood & Cellulose
pMC
Dr. E. M. Scott, U. Glasgow
IAEA-315 (*)
Marine Sediment
Radionuclides
IAEA (4)
IAEA-356 (*)
Polluted Marine Sediment
Trace Elements & Methyl Mercury
IAEA
IAEA-368 (*)
Marine Sediment
Radionuclides
IAEA
IAEA-381
Natural Seawater
Radionuclides
IAEA
IAEA-383 (*)
Marine Sediment
Organic Contaminants
IAEA
IAEA-384 (*)
Lagoon Sediment
Radionuclides
IAEA (available soon)
IAEA-408 (*)
Marine Sediment
Organic Contaminants
IAEA
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Chemical Reference Materials: Setting the Standards for Ocean Science
Identifier
Matrix
Analyzed For
Source (see footnotes)
IAEA-C1
Carrara Marble
δ13C, pMC
IAEA
IAEA-C2
Freshwater Travertine
δ13C, pMC
IAEA
IAEA-C3
Cellulose, 1989 Growth of Tree
δ13C, pMC
IAEA
IAEA-C5
Sub-fossil Wood E. Wisconsin Forest
δ13C, pMC
IAEA
IAEA-C6
Sucrose (ANU)
δ13C, pMC
IAEA
IAEA-CO-1
CaCO3 (Carrara Marble)
δ13C
IAEA
IAEA-CO-8
(IAEA-KST)
CaCO3 (Calcite)
δ13C
IAEA
IAEA-CO-9
(IAEA-NZCH)
Barium Carbonate
δ13C
IAEA
LSVEC
SRM 8455
Lithium Carbonate
δ13C
IAEA (out of stock at NIST)
SRM 1648 (*)
Urban Atmospheric Particulate
Trace Elements
NIST(5)
SRM 1649A (*)
Urban Dust
Organic Constituents
NIST
SRM 1650A (*)
Diesel Particulate
Organic Constituents
NIST (being replaced)
SRM 1939 (*)
River Sediment
PCBs & Chlorinated Pesticides
NIST
SRM 1941B (*)
Marine Sediment
Various Organics
NIST (in prep.)
SRM 1944 (*)
New York/New Jersey Waterway Sediment
Various Organics
NIST
SRM 1945 (*)
Whale Blubber
PCBs & Chlorinated Pesticides
NIST
SRM 4321C
1 M HNO3
238U, 235U, 234U
NIST
SRM 4325
BeCl2 solution
10Be/9Be
NIST
SRM 4339B
1.4 M HCl ?
228Ra
NIST (in prep.)
SRM 4350B
River Sediment
Radionuclides
NIST
SRM 4357
Marine Sediment
Radionuclides
NIST
SRM 4361C
Water
3H
NIST
SRM 4969
1.5 M HCl
226Ra
NIST
SRM 4990C
Oxalic Acid Powder
14C
NIST
RM 8452
Sucrose (ANU)
δ13C, pMC
NIST
SRM 8454
CaCO3
δ13C, δ18O
NIST, IAEA
NBS 19 (TS-limestone)
RM 8539
Oil
δ2H, δ13C
NIST, IAEA
NBS 22
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Chemical Reference Materials: Setting the Standards for Ocean Science
Identifier
Matrix
Analyzed For
Source (see footnotes)
RM 8540 PEF1
Polyethylene
δ2H, δ13C
NIST, IAEA
IAEA-CH-7
RM 8541
C (graphite)
δ13C
NIST, IAEA
USGS24
RM 8562
CO2 gas
δ13C
NIST, IAEA
RM 8563
CO2 gas
δ13C
NIST, IAEA
RM 8564
CO2 gas
δ13C
NIST, IAEA
IAEA-NGS1
Natural Gas (Coal)
δ2H, d13C
NIST-ACG(6)
IAEA-NGS2
Natural Gas (Oil)
δ2H, d13C
NIST-ACG
IAEA-NGS3
Natural Gas (Biogenic)
δ2H, δ13C
NIST-ACG
HISS-1 (*)
Marine Sediment
Trace Metals
NRC-IMB, Canada(7)
HS-3B (*)
Harbor Sediment
Polycyclic Aromatic Hydrocarbons
NRC-IMB, Canada
HS-4B (*)
Harbor Sediment
Polycyclic Aromatic Hydrocarbons
NRC-IMB, Canada
HS-5 (*)
Harbor Sediment
Polycyclic Aromatic Hydrocarbons
NRC-IMB, Canada
HS-6 (*)
Harbor Sediment
Polycyclic Aromatic Hydrocarbons
NRC-IMB, Canada
SES-1 (*)
Estuarine Sediment
Polycyclic Aromatic Hydrocarbons
NRC-IMB, Canada
CARP-2 (*)
Ground Whole Carp
Organochlorine Compounds
NRC-INMS, Canada(8)
DOLT-2 (*)
Dogfish Liver
Trace Metals
NRC-INMS, Canada
DORM-2 (*)
Dogfish Muscle
Trace Metals
NRC-INMS, Canada
LUTS-1 (*)
Non-defatted Lobster Hepatopancreas
Trace Metals
NRC-INMS, Canada
MESS-3 (*)
Marine Sediment
Trace Metals
NRC-INMS, Canada
NASS-5
Natural Seawater
Trace Metals
NRC-INMS, Canada
PACS-2 (*)
Marine Sediment
Trace Metals
NRC-INMS, Canada
TORT-2 (*)
Lobster Hepatopancreas
Trace Metals
NRC-INMS, Canada
IAPSO Standard Seawater
Natural Seawater
Salinity
Ocean Scientific International Ltd.(9)
CSK Standard Solutions (various)
3.05% NaCl Solution
Nitrate, nitrite, phosphate, silicate
Wako Pure Chemical Industries(10)
CSK Standard Solution
Potassium Iodate (0.0100N)
For oxygen titration
Wako Pure Chemical Industries
MAG-1 (*)
Marine Sediment
Elemental Composition
USGS(11)
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Chemical Reference Materials: Setting the Standards for Ocean Science
Table Footnotes
†4th International Radiocarbon Intercomparison (Bryant et al., 2001; Boaretto et al., in press): http://www.stats.gla.ac.uk/~marian/intercomp.html
*These RMs were suggested in Table 4.2 as materials that could be useful for organic analyses (though not explicitly designed for such constituents).
Sources for RMs mentioned in Table:
(1) Dr. Andrew Dickson: http://www-mpl.ucsd.edu/people/adickson/CO2_QC/ (Contact: co2rms@mpl.ucsd.edu)
(2) Dr. Dennis Hansell: http://www.bbsr.edu/Labs/hanselllab/crm.html (Contact: wenchen@rsmas.miami.edu)
(3) Prof E M Scott, Dept of Statistics, University of Glasgow, Glasgow G12 8QW UK (marian@stats.gla.ac.uk)
(4) IAEA: http://www.iaea.org/programmes/aqcs/
(5) NIST: http://ts.nist.gov/ts/htdocs/230/232/232.htm
(6) NIST Atmospheric Chemistry Group: http://www.cstl.nist.gov/div837/837.01/outputs/standards/StdMat.htm
(7) NRC-IMB, Canada: http://www.imb.nrc.ca/crmp_e.html
(8) NRC-INMS, Canada: http://www.ems.nrc.ca/ems1.htm
(9) Ocean Scientific: http://www.oceanscientific.com/seawaterdivision.htm
(10) Although these were originally distributed by the Sagami Chemical Research Center, they are now available from Wako Pure Chemical Industries through their on-line catalog (Keyword: CSK): http://www.wako-chem.co.jp/specialty/
(11) U.S. Geological Survey: http://minerals.cr.usgs.gov/geo_chem_stand/
Additional sources for Reference Materials:
(1) A limited selection of environmental reference materials is also available from the European Institute for Reference Materials and Measurements in Belgium: http://www.irmm.jrc.be/
(2) International Steering Committee for Black Carbon Reference http://www.du.edu/~dwismith/bcsteer.html
Representative terms from entire chapter:
ocean science
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